预变形对超高强铝合金挤压材组织性能的影响
发布人：上海艾荔艾合金股份有限公司www.shailiai.cn
更新时间：2016-04-01
采用硬度与电导率测试、拉伸试验、晶间腐蚀和剥落腐蚀试验以及X射线衍射(XRD)、扫描电镜(SEM)、电子背散射衍射(EBSD)分析等方法研究预变形对Al-12.45Zn-3.56Mg-1.12Cu-0.21Zr-0.0553Sr铝合金挤压材组织与性能的影响。
预变形对超高强铝合金挤压材组织性能的影响Effect of pre-deformation on microstructure and properties of ultra-high strength aluminum alloy extrusion materials采用硬度与电导率测试、拉伸试验、晶间腐蚀和剥落腐蚀试验以及X射线衍射(XRD)、扫描电镜(SEM)、电子背散射衍射(EBSD)分析等方法研究预变形对Al-12.45Zn-3.56Mg-1.12Cu-0.21Zr-0.0553Sr铝合金挤压材组织与性能的影响。结果表明：该合金在(121 ℃, 24 h)时效制度下，预变形处理能有效引入位错，位错密度从0.197×10-14 m-2提高到1.156×10-14 m-2；同时，由于位错对强度的贡献高达58.7 MPa。根据EBSD分析，经预变形处理后，合金的低角度晶界所占比例为66.2%，比未经预变形处理的合金提高12.6%，平均晶界角度值降低3.894°，平均晶粒尺寸增长6.396 mm。预变形能够明显提高合金的抗晶间腐蚀性能(最大晶间腐蚀深度由222.1 mm降低至165 mm)，对剥落腐蚀性能的影响不明显。
The effects of pre-deformation on microstructure and properties of Al-12.45Zn-3.56Mg-1.12Cu-0.21Zr- 0.0553Sr ultra-high strength aluminum alloy extrusion materials were studied by means of micro-hardness tester and electrical conductivity test, tensile test, intergranular and exfoliation corrosion experiment, X-ray diffraction (XRD), scanning electron microscopy (SEM) and electron back-scattered diffraction (EBSD) analysis. The results show that in the aging system at 121 ℃ for 24 h, the pre-deformation can effectively introduce dislocations,the dislocation density increases from 0.197×10-14 m-2to 1.156×10-14 m-2, and the strength reaches up to 58.7 MPa because of the dislocation contribution.Based on EBSD analysis, after pre-deformation treatment, the low angle grain boundary proportion (66.2%) of the pre-deformation alloy increases by 12.6% than that of the underformed alloy, the mean misorientation value reduces 3.894°, and the average grain size increases by 6.396 μm. The pre-deformation treatment can significantly improve the intergranular corrosion resistance properties (the maximum intergranular corrosion depth reducing from 222.1 μm to 165 μm), but little improvement on exfoliation corrosion performance.
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