保温时间对K452高温合金钎焊接头组织与性能的影响Effect of Holding Time on Microstructure and Mechanical Properties of K452 Superalloy Brazed Joints

采用钴基钎料及镍基合金粉料,分别在1170℃保温10min、60min和120min的钎焊工艺下,对K452镍基铸造高温合金进行真空钎焊实验,通过扫描电镜和能谱分析仪进行了接头显微组织观察与物相分析,并测试钎焊接头的高温力学性能。结果表明:在保温60min的工艺规范下,界面实现较好的结合,钎缝内部孔洞缺陷较少,钎缝组织均匀,有利于钎焊接头性能的提高;在更长的保温时间120min下,钎缝内部又有蚀孔缺陷形成,且较多的白色块状化合物在合金粉颗粒间聚集长大,但界面结合良好,钎焊接头性能较高,900℃抗拉强度达到400MPa,900℃/100MPa持久寿命为141h55min。

Vacuum brazing of K452 superalloy was performed with cobalt-base filler metal and nickel-base superalloy powder under brazing conditions of 1170℃/10min, 1170℃/60min and 1170℃/120min respectively. The microstructure of brazed joints was analyzed by using SEM and EDS, and the high-temperature mechanical properties were also studied. The results show that the sound joints with fine microstructure and rare pores are achieved under 1170℃/60min brazing procedure, due to the good quality of interface. The joints braze under 1170℃/120min show the highest mechanical properties because of better interface quality, the average 900℃ tensile strength of 400MPa and 900℃/100MPa stress-rupture life of 141h/55min. But there morepoles are presented, and many white particles of compound congregated and grow up between the nickel-base superalloy powder in the brazing seam.